Green Synthesis of Tin Based Nano Medicine: Assessment of Microstructure and Surface Property

Sethumadhavan Sudhaparimala; Arumugam Gnanamani A.; Asit Baran Mandal

doi:doi:10.11648/j.nano.20140204.13

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Green Synthesis of Tin Based Nano Medicine: Assessment of Microstructure and Surface Property

Sethumadhavan Sudhaparimala, Arumugam Gnanamani A., Asit Baran Mandal

Published in American Journal of Nanoscience and Nanotechnology (Volume 2, Issue 4)

Received: 4 June 2014 Accepted: 22 July 2014 Published: 10 August 2014

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Abstract

The present study is about an eco-friendly and cost effective method of using five potent plant extracts and sunlight as the reaction medium and grinding as a nano technique to prepare nano composite of tin (IV) oxide from tin metal. The equivalent preparation is widely used as a drug formulation in the treatment of spectrum of infectious diseases. The intensive grinding and calcinations with the plant material lead to the formation of nano crystallite with a tetragonal phase with an average crystallite size of 27nm. The elements Ca, P, Na, Mg and Fe at the microscopic level identified at the surface of the nano crystallite by the X – ray Photo Electron Spectroscopy showed the uniqueness of the synthesis. The formation of spherical crystallites with good distribution of pores was indicated by the electron microscopic images and adsorption studies. The presence of oxygen deficiency arising due to nonstoichiometry in the crystal lattice was evident from the Electron paramagnetic Resonance study. The free radical equivalent of DPPH radical calculated for the final stage sample was suggestive of its anti-oxidant property and hence it’s biological activity. The overall research study provided an alternative route of preparing nontoxic nano tin (IV) oxide composite with good biological activity apart from its already proven catalytic and sensor applications.

Published in	American Journal of Nanoscience and Nanotechnology (Volume 2, Issue 4)
DOI	10.11648/j.nano.20140204.13
Page(s)	75-83
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2014. Published by Science Publishing Group

Keywords

Nanomedicine, Green Synthesis, Nano Tin (IV) Oxide Composite, Microstructure

References

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APA Style

Sethumadhavan Sudhaparimala, Arumugam Gnanamani A., Asit Baran Mandal. (2014). Green Synthesis of Tin Based Nano Medicine: Assessment of Microstructure and Surface Property. American Journal of Nano Research and Applications, 2(4), 75-83. https://doi.org/10.11648/j.nano.20140204.13

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ACS Style

Sethumadhavan Sudhaparimala; Arumugam Gnanamani A.; Asit Baran Mandal. Green Synthesis of Tin Based Nano Medicine: Assessment of Microstructure and Surface Property. Am. J. Nano Res. Appl. 2014, 2(4), 75-83. doi: 10.11648/j.nano.20140204.13

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AMA Style

Sethumadhavan Sudhaparimala, Arumugam Gnanamani A., Asit Baran Mandal. Green Synthesis of Tin Based Nano Medicine: Assessment of Microstructure and Surface Property. Am J Nano Res Appl. 2014;2(4):75-83. doi: 10.11648/j.nano.20140204.13

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@article{10.11648/j.nano.20140204.13,
  author = {Sethumadhavan Sudhaparimala and Arumugam Gnanamani A. and Asit Baran Mandal},
  title = {Green Synthesis of Tin Based Nano Medicine: Assessment of Microstructure and Surface Property},
  journal = {American Journal of Nano Research and Applications},
  volume = {2},
  number = {4},
  pages = {75-83},
  doi = {10.11648/j.nano.20140204.13},
  url = {https://doi.org/10.11648/j.nano.20140204.13},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.nano.20140204.13},
  abstract = {The present study is about an eco-friendly and cost effective method of using five potent plant extracts and sunlight as the reaction medium and grinding as a nano technique to prepare nano composite of tin (IV) oxide from tin metal. The equivalent preparation is widely used as a drug formulation in the treatment of spectrum of infectious diseases. The intensive grinding and calcinations with the plant material lead to the formation of nano crystallite with a tetragonal phase with an average crystallite size of 27nm. The elements Ca, P, Na, Mg and Fe at the microscopic level identified at the surface of the nano crystallite by the X – ray Photo Electron Spectroscopy showed the uniqueness of the synthesis. The formation of spherical crystallites with good distribution of pores was indicated by the electron microscopic images and adsorption studies. The presence of oxygen deficiency arising due to nonstoichiometry in the crystal lattice was evident from the Electron paramagnetic Resonance study. The free radical equivalent of DPPH radical calculated for the final stage sample was suggestive of its anti-oxidant property and hence it’s biological activity. The overall research study provided an alternative route of preparing nontoxic nano tin (IV) oxide composite with good biological activity apart from its already proven catalytic and sensor applications.},
 year = {2014}
}

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TY  - JOUR
T1  - Green Synthesis of Tin Based Nano Medicine: Assessment of Microstructure and Surface Property
AU  - Sethumadhavan Sudhaparimala
AU  - Arumugam Gnanamani A.
AU  - Asit Baran Mandal
Y1  - 2014/08/10
PY  - 2014
N1  - https://doi.org/10.11648/j.nano.20140204.13
DO  - 10.11648/j.nano.20140204.13
T2  - American Journal of Nano Research and Applications
JF  - American Journal of Nano Research and Applications
JO  - American Journal of Nano Research and Applications
SP  - 75
EP  - 83
PB  - Science Publishing Group
SN  - 2575-3738
UR  - https://doi.org/10.11648/j.nano.20140204.13
AB  - The present study is about an eco-friendly and cost effective method of using five potent plant extracts and sunlight as the reaction medium and grinding as a nano technique to prepare nano composite of tin (IV) oxide from tin metal. The equivalent preparation is widely used as a drug formulation in the treatment of spectrum of infectious diseases. The intensive grinding and calcinations with the plant material lead to the formation of nano crystallite with a tetragonal phase with an average crystallite size of 27nm. The elements Ca, P, Na, Mg and Fe at the microscopic level identified at the surface of the nano crystallite by the X – ray Photo Electron Spectroscopy showed the uniqueness of the synthesis. The formation of spherical crystallites with good distribution of pores was indicated by the electron microscopic images and adsorption studies. The presence of oxygen deficiency arising due to nonstoichiometry in the crystal lattice was evident from the Electron paramagnetic Resonance study. The free radical equivalent of DPPH radical calculated for the final stage sample was suggestive of its anti-oxidant property and hence it’s biological activity. The overall research study provided an alternative route of preparing nontoxic nano tin (IV) oxide composite with good biological activity apart from its already proven catalytic and sensor applications.
VL  - 2
IS  - 4
ER  -

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Author Information

Sethumadhavan Sudhaparimala

Department of Chemistry, Ethiraj College for Women (Autonomous), Chennai – 8, India
Arumugam Gnanamani A.

Microbiology Division, Central Leather Research Institute (CSIR, New Delhi), Adyar, Chennai 20, India
Asit Baran Mandal

Chemical Laboratory, Central Leather Research Institute, Adyar, Chennai (Madras) 600020, India

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APA Style

Sethumadhavan Sudhaparimala, Arumugam Gnanamani A., Asit Baran Mandal. (2014). Green Synthesis of Tin Based Nano Medicine: Assessment of Microstructure and Surface Property. American Journal of Nano Research and Applications, 2(4), 75-83. https://doi.org/10.11648/j.nano.20140204.13

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ACS Style

Sethumadhavan Sudhaparimala; Arumugam Gnanamani A.; Asit Baran Mandal. Green Synthesis of Tin Based Nano Medicine: Assessment of Microstructure and Surface Property. Am. J. Nano Res. Appl. 2014, 2(4), 75-83. doi: 10.11648/j.nano.20140204.13

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AMA Style

Sethumadhavan Sudhaparimala, Arumugam Gnanamani A., Asit Baran Mandal. Green Synthesis of Tin Based Nano Medicine: Assessment of Microstructure and Surface Property. Am J Nano Res Appl. 2014;2(4):75-83. doi: 10.11648/j.nano.20140204.13

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@article{10.11648/j.nano.20140204.13,
  author = {Sethumadhavan Sudhaparimala and Arumugam Gnanamani A. and Asit Baran Mandal},
  title = {Green Synthesis of Tin Based Nano Medicine: Assessment of Microstructure and Surface Property},
  journal = {American Journal of Nano Research and Applications},
  volume = {2},
  number = {4},
  pages = {75-83},
  doi = {10.11648/j.nano.20140204.13},
  url = {https://doi.org/10.11648/j.nano.20140204.13},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.nano.20140204.13},
  abstract = {The present study is about an eco-friendly and cost effective method of using five potent plant extracts and sunlight as the reaction medium and grinding as a nano technique to prepare nano composite of tin (IV) oxide from tin metal. The equivalent preparation is widely used as a drug formulation in the treatment of spectrum of infectious diseases. The intensive grinding and calcinations with the plant material lead to the formation of nano crystallite with a tetragonal phase with an average crystallite size of 27nm. The elements Ca, P, Na, Mg and Fe at the microscopic level identified at the surface of the nano crystallite by the X – ray Photo Electron Spectroscopy showed the uniqueness of the synthesis. The formation of spherical crystallites with good distribution of pores was indicated by the electron microscopic images and adsorption studies. The presence of oxygen deficiency arising due to nonstoichiometry in the crystal lattice was evident from the Electron paramagnetic Resonance study. The free radical equivalent of DPPH radical calculated for the final stage sample was suggestive of its anti-oxidant property and hence it’s biological activity. The overall research study provided an alternative route of preparing nontoxic nano tin (IV) oxide composite with good biological activity apart from its already proven catalytic and sensor applications.},
 year = {2014}
}

Copy | Download

TY  - JOUR
T1  - Green Synthesis of Tin Based Nano Medicine: Assessment of Microstructure and Surface Property
AU  - Sethumadhavan Sudhaparimala
AU  - Arumugam Gnanamani A.
AU  - Asit Baran Mandal
Y1  - 2014/08/10
PY  - 2014
N1  - https://doi.org/10.11648/j.nano.20140204.13
DO  - 10.11648/j.nano.20140204.13
T2  - American Journal of Nano Research and Applications
JF  - American Journal of Nano Research and Applications
JO  - American Journal of Nano Research and Applications
SP  - 75
EP  - 83
PB  - Science Publishing Group
SN  - 2575-3738
UR  - https://doi.org/10.11648/j.nano.20140204.13
AB  - The present study is about an eco-friendly and cost effective method of using five potent plant extracts and sunlight as the reaction medium and grinding as a nano technique to prepare nano composite of tin (IV) oxide from tin metal. The equivalent preparation is widely used as a drug formulation in the treatment of spectrum of infectious diseases. The intensive grinding and calcinations with the plant material lead to the formation of nano crystallite with a tetragonal phase with an average crystallite size of 27nm. The elements Ca, P, Na, Mg and Fe at the microscopic level identified at the surface of the nano crystallite by the X – ray Photo Electron Spectroscopy showed the uniqueness of the synthesis. The formation of spherical crystallites with good distribution of pores was indicated by the electron microscopic images and adsorption studies. The presence of oxygen deficiency arising due to nonstoichiometry in the crystal lattice was evident from the Electron paramagnetic Resonance study. The free radical equivalent of DPPH radical calculated for the final stage sample was suggestive of its anti-oxidant property and hence it’s biological activity. The overall research study provided an alternative route of preparing nontoxic nano tin (IV) oxide composite with good biological activity apart from its already proven catalytic and sensor applications.
VL  - 2
IS  - 4
ER  -

Copy | Download